As a general rule I would agree with >>11537 but on the flipside, when doing a compound exercise, you might (subconsciously) shift the load so that a dominant muscle takes the brunt of the load. Doing an isometric exercise targeting that muscle first may help you work out the lesser muscles better. I guess it's a question of form; If you have perfect form this issue is moot and you should go with compounds first. Worth keeping in mind just in case, though.
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